Brookfield DV2+Pro Viscometer Bedienungsanleitung

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Brookeld Engineering Labs., Inc. Page 1 Manual No. M03-165-F0612
SPECIALISTS IN THE
MEASUREMENT AND
CONTROL OF VISCOSITY
TEL 508-946-6200
F
AX 508-946-6262
or 800-628-8139 (USA excluding MA)
I
NTERNET
http://www.brookeldengineering.com
BROOKFIELD ENGINEERING LABORATORIES, INC.
11 Commerce Boulevard, Middleboro, MA 02346 USA
with oces in :
Boston • Chicago • London • Stuttgart • Guangzhou
BROOKFIELD DV-II+Pro
Viscometer
Operating Instructions
Manual No. M03-165-F0612
Seitenansicht 0
1 2 3 4 5 6 ... 100 101

Inhaltsverzeichnis

Seite 1 - BROOKFIELD DV-II+Pro

Brookeld Engineering Labs., Inc. Page 1 Manual No. M03-165-F0612 SPECIALISTS IN THE MEASUREMENT AND CONTROL OF VISCOSITY TEL 508-946-6200F

Seite 2

Brookeld Engineering Labs., Inc. Page 10 Manual No. M03-165-F0612 3) Connect the RTD probe to the socket on the rear panel of the DV-II+Pro.

Seite 3 - Table of Contents

Brookeld Engineering Labs., Inc. Page 100 Manual No. M03-165-F0612Appendix N - Warranty Repair and ServiceWarrantyBrookeldViscometersaregua

Seite 4

BROOKFIELD ENGINEERING LABORATORIES, INC. • 11 Commerce Blvd. • Middleboro, MA 02346 • TEL: 508-946-6200 or 800-628-8139 FAX: 508-946-6262 • www.brook

Seite 5 - I. INTRODUCTION

Brookeld Engineering Labs., Inc. Page 11 Manual No. M03-165-F0612 In case of emergency, turn off the instrument and then disconnect the electri

Seite 6

Brookeld Engineering Labs., Inc. Page 12 Manual No. M03-165-F0612 SELECT SPINDLE  Initiatesspindleselectionontherstpressandthen

Seite 7 - COMPONENT DIAGRAM

Brookeld Engineering Labs., Inc. Page 13 Manual No. M03-165-F0612II. GETTING STARTED II.1 AutozeroBefore readings may be taken, the Viscomete

Seite 8

Brookeld Engineering Labs., Inc. Page 14 Manual No. M03-165-F0612 The display will vary depending upon the selection of temperature (°F or °C)

Seite 9

Brookeld Engineering Labs., Inc. Page 15 Manual No. M03-165-F0612Note: TheDV-II+Pro will remember the Spindle Entry Code which was in use whe

Seite 10

Brookeld Engineering Labs., Inc. Page 16 Manual No. M03-165-F0612how to install a Custom Speed Set.ToselectaViscometerspeedrstpresseith

Seite 11 - BROOKFIELD

Brookeld Engineering Labs., Inc. Page 17 Manual No. M03-165-F0612cP 0.0 20.1COFFRPM % 0.0Figure II-10Pressing the MOTOR ON/OFF/ESCAPE key a

Seite 12 - CGS UNITS #

Brookeld Engineering Labs., Inc. Page 18 Manual No. M03-165-F0612SR 40.0 20.1C6.0RPM % 15.6Figure II-13OnemorepressoftheSELECTDISPLAY

Seite 13 - +Pro defaultscreen:

Brookeld Engineering Labs., Inc. Page 19 Manual No. M03-165-F0612 II.6 Out of Range The DV-II+Pro gives indications for out-of-range operati

Seite 15

Brookeld Engineering Labs., Inc. Page 20 Manual No. M03-165-F0612 II.7 Temperature Display The DV-II+Pro displays the measured temperature w

Seite 16 - Figure II-9

Brookeld Engineering Labs., Inc. Page 21 Manual No. M03-165-F0612 Tostopcontinuous printing, press the PRINTkey forone(1)second. 

Seite 17 - Figure II-12

Brookeld Engineering Labs., Inc. Page 22 Manual No. M03-165-F0612 The DV-II+Pro may be set to stand alone mode by turning it OFF and ON again

Seite 18 - Figure II-14

Brookeld Engineering Labs., Inc. Page 23 Manual No. M03-165-F0612maximum accuracy, readings below 10% should be avoided. Record values. 4. P

Seite 19 - Figure II-18

Brookeld Engineering Labs., Inc. Page 24 Manual No. M03-165-F0612III. MAKING VISCOSITY MEASUREMENTS III.1 Quick StartThe DV-II+Pro Viscomete

Seite 20 - Figure II-20

Brookeld Engineering Labs., Inc. Page 25 Manual No. M03-165-F0612 Please see our publication, “More Solutions to Sticky Problems”, for more

Seite 21 - Figure II-24

Brookeld Engineering Labs., Inc. Page 26 Manual No. M03-165-F0612IV. OPTIONS IV.1 OPTIONTABFIntroduction to OPTIONS The OPTIONS/TAB keyprovid

Seite 22

Brookeld Engineering Labs., Inc. Page 27 Manual No. M03-165-F0612 ENTERAUTORANGE ENTER/AUTORANGE -Acceptsthecurrently

Seite 23

Brookeld Engineering Labs., Inc. Page 28 Manual No. M03-165-F0612On entry to the Options menu, the following rules regarding current viscometer

Seite 24

Brookeld Engineering Labs., Inc. Page 29 Manual No. M03-165-F0612DCGS UNITS #DCUSTOM SPEEDS $$#1111D°F(FAHRENHEIT) #DCGS UNITS $D°F(FAHRENH

Seite 25

Brookeld Engineering Labs., Inc. Page 3 Manual No. M03-165-F0612Table of ContentsI. INTRODUCTION ...

Seite 26 - IV. OPTIONS

Brookeld Engineering Labs., Inc. Page 30 Manual No. M03-165-F0612D°F(FAHRENHEIT) DCGS UNITS D°C(CENTIGRADE) DCGS UNITS "Figure IV-5To sele

Seite 27

Brookeld Engineering Labs., Inc. Page 31 Manual No. M03-165-F0612AUTORANGEkeytoselecttheashingoption.ÉDCGS UNITS DSEQUENTIALê1DCGS UNITS

Seite 28 - Figure IV-2

Brookeld Engineering Labs., Inc. Page 32 Manual No. M03-165-F0612Pressing the OPTIONS/TAB key “toggles” between the two port choices. To selec

Seite 29 - Figure IV-4

Brookeld Engineering Labs., Inc. Page 33 Manual No. M03-165-F0612 IV.3 Time ModesTheTimeModesareprovidedtoallowmoreexibilitybyuna

Seite 30

Brookeld Engineering Labs., Inc. Page 34 Manual No. M03-165-F0612TIMED STOPSET SEC’S: 00 ↑↓ Figure IV-17Using the UP and DOWN ARROW keys, the

Seite 31

Brookeld Engineering Labs., Inc. Page 35 Manual No. M03-165-F0612cP 123.5e6MIN: 15 SEC: 13Figure IV-20Note: When this mode has begun, a press

Seite 32

Brookeld Engineering Labs., Inc. Page 36 Manual No. M03-165-F0612 IV.3.2 Time to TorqueOnentrytothismode,theuserispresentedwithth

Seite 33 - Figure IV-16

Brookeld Engineering Labs., Inc. Page 37 Manual No. M03-165-F0612TORQUE = 24.2%MIN: 15 SEC: 13 Figure IV-26Note: When this mode has beg

Seite 34

Brookeld Engineering Labs., Inc. Page 38 Manual No. M03-165-F0612printmodeandnallyinitiateeitherofthetimedmodesofoperation.While

Seite 35

Brookeld Engineering Labs., Inc. Page 39 Manual No. M03-165-F0612Activating print selections in the Print mode can only be done by exiting to t

Seite 36 - Figure IV-24

IV.3.5 Download a Program ...40 I

Seite 37

Brookeld Engineering Labs., Inc. Page 40 Manual No. M03-165-F0612 IV.3.5 Download a ProgramPlease refer to Section V for details on how to c

Seite 38

Brookeld Engineering Labs., Inc. Page 41 Manual No. M03-165-F0612A press of any key (except the MOTOR ON/OFF/ESCAPE key) will take the user bac

Seite 39

Brookeld Engineering Labs., Inc. Page 42 Manual No. M03-165-F0612where the operator is instructed to mount a spindle 31 and then press a key to

Seite 40

Brookeld Engineering Labs., Inc. Page 43 Manual No. M03-165-F0612V. DVLOADER SOFTWAREThe DVLOADER software is a WINDOWS-based program provided

Seite 41

Brookeld Engineering Labs., Inc. Page 44 Manual No. M03-165-F0612 SSP Two digit spindle code Calculations of viscosity, shear stress, and sh

Seite 42 - Figure IV-44

Brookeld Engineering Labs., Inc. Page 45 Manual No. M03-165-F0612Figure IV-2 shows the grid where the operator programs are created. It is use

Seite 43 - V. DVLOADER SOFTWARE

Brookeld Engineering Labs., Inc. Page 46 Manual No. M03-165-F0612Click the Delete button to delete the B.E.V.I.S. command in the selected row o

Seite 44 - Figure IV-1

Brookeld Engineering Labs., Inc. Page 47 Manual No. M03-165-F0612 V.5 Example ProgramsThe following example programs can also be found on th

Seite 45

Brookeld Engineering Labs., Inc. Page 48 Manual No. M03-165-F0612Command Command Description Parameter CommentsWPT Wait for % torque 85.0 wait

Seite 46 -  • Set PC PROG to “OFF.”

Brookeld Engineering Labs., Inc. Page 49 Manual No. M03-165-F0612VI. AUTOMATED DATA GATHERING & ANALYSISTherearetwochoicesofapplicati

Seite 47

Brookeld Engineering Labs., Inc. Page 5 Manual No. M03-165-F0612I. INTRODUCTIONTheBrookeldDV-II+ProViscometermeasuresuidviscosityatgi

Seite 48

Brookeld Engineering Labs., Inc. Page 50 Manual No. M03-165-F0612Figure V1-2: Gather ScreenFigure V1-3: DV Loader Screen

Seite 49

Brookeld Engineering Labs., Inc. Page 51 Manual No. M03-165-F0612Figure V1-4: Run/Data ScreenFigure V1-5: Analysis Screen

Seite 50 - Figure V1-3: DV Loader Screen

Brookeld Engineering Labs., Inc. Page 52 Manual No. M03-165-F0612 Figure V1-6: Setup Screen Figure V1-7: Custom Screen

Seite 51 - Figure V1-5: Analysis Screen

Brookeld Engineering Labs., Inc. Page 53 Manual No. M03-165-F0612 V1.2 RheocalcImportantfeaturesandbenetsinRheocalcwhichenhanceoper

Seite 52 - Figure V1-7: Custom Screen

Brookeld Engineering Labs., Inc. Page 54 Manual No. M03-165-F0612Figure V1-9: Test ScreenFigure V1-10: Run/Data Screen

Seite 53 - Figure V1-8: Dashboard Screen

Brookeld Engineering Labs., Inc. Page 55 Manual No. M03-165-F0612Figure V1-11: Setup ScreenFigure V1-12: Analysis Screen

Seite 54 - Figure V1-10: Run/Data Screen

Brookeld Engineering Labs., Inc. Page 56 Manual No. M03-165-F0612Figure V1-13: Custom Screen V1.3 Math ModelsNote: Someorallofthesemod

Seite 55 - Figure V1-12: Analysis Screen

Brookeld Engineering Labs., Inc. Page 57 Manual No. M03-165-F0612V1.3.1 The Power Law (Ostwald) Modelτ = kn ( τ=shearstress,k=consi

Seite 56 - Figure V1-13: Custom Screen

Brookeld Engineering Labs., Inc. Page 58 Manual No. M03-165-F0612 An Example of the Power Law Model at WorkFormulators at a personal care comp

Seite 57 - Figure V1-14

Brookeld Engineering Labs., Inc. Page 59 Manual No. M03-165-F0612 Figure V1-15When should you use it?The Herschel-Bulkley

Seite 58 - =shearstress

Brookeld Engineering Labs., Inc. Page 6 Manual No. M03-165-F0612TheequivalentunitsofmeasurementintheSIsystemarecalculatedusingthef

Seite 59

Brookeld Engineering Labs., Inc. Page 60 Manual No. M03-165-F0612V1.3.3 The Bingham Model τ=τ° + hD ( =shearstress, τ° =yieldst

Seite 60

Brookeld Engineering Labs., Inc. Page 61 Manual No. M03-165-F0612 An Example of the Bingham Model at WorkA manufacturer of drilling uid

Seite 61 - τ=shearstress

Brookeld Engineering Labs., Inc. Page 62 Manual No. M03-165-F0612When should you use it?The Casson model should be used with non-Newtonian mate

Seite 62

Brookeld Engineering Labs., Inc. Page 63 Manual No. M03-165-F0612V1.3.5 Other Common Rheological ModelsThe NCA/CMA Casson Model(1 + a) √τ

Seite 63 - √τ = 2√τ + (1 + a) √ηγ

Brookeld Engineering Labs., Inc. Page 64 Manual No. M03-165-F0612This model is a variation of the Power Law Model. Unlike the Power Law Model,

Seite 64

Brookeld Engineering Labs., Inc. Page 65 Manual No. M03-165-F0612Appendix A - Cone/Plate Viscometer Set-UpThis Cone/Plate version of the DV-II+

Seite 65 - Figure A-1

Brookeld Engineering Labs., Inc. Page 66 Manual No. M03-165-F0612 A.2 Setup1. Be sure that the Viscometer is securely mounted to the Laborat

Seite 66 - Note: Left Hand Threads

Brookeld Engineering Labs., Inc. Page 67 Manual No. M03-165-F0612 A.3 Setting the Gap1. Move the toggle switch to the right; this will turn

Seite 67 - Figure A-6

Brookeld Engineering Labs., Inc. Page 68 Manual No. M03-165-F0612 A.4 Verifying Calibration1. Determine the appropriate sample volume. Refe

Seite 68

Brookeld Engineering Labs., Inc. Page 69 Manual No. M03-165-F0612Appendix B - Viscosity RangesViscosity Range TablesViscosity ranges shown are

Seite 69 - Appendix B - Viscosity Ranges

Brookeld Engineering Labs., Inc. Page 7 Manual No. M03-165-F0612COMPONENT DIAGRAMCone/Plate OptionTemperature ProbeSpindle SetCone SpindleWrenc

Seite 70

Brookeld Engineering Labs., Inc. Page 70 Manual No. M03-165-F0612UL AdapterUL SpindleViscosity (cP)Shear Rate sec-1LVDV-II+ RVDV-II+ HADV-II+ H

Seite 71 - Pa=Pascal

Brookeld Engineering Labs., Inc. Page 71 Manual No. M03-165-F0612Vane SpindlesSpindle Torque RangeShear Stress Range (Pa)Viscosity Range cP (mP

Seite 72

Brookeld Engineering Labs., Inc. Page 72 Manual No. M03-165-F0612Special ConsiderationsIn taking viscosity measurements with the DV-II+Pro Visc

Seite 73

Brookeld Engineering Labs., Inc. Page 73 Manual No. M03-165-F0612sample introduction techniques. The effect of these elements on measurement t

Seite 74

Brookeld Engineering Labs., Inc. Page 74 Manual No. M03-165-F0612Appendix C - Variables in Viscosity MeasurementsAs with any instrument measure

Seite 75

Brookeld Engineering Labs., Inc. Page 75 Manual No. M03-165-F0612Theshearrateofagivenmeasurementisdeterminedby:therotationalspeed

Seite 76 - Table D-1 (Continued)

Brookeld Engineering Labs., Inc. Page 76 Manual No. M03-165-F0612Appendix D - Spindle and Model CodesEach spindle has a two digit entry code wh

Seite 77 - Table D-1

Brookeld Engineering Labs., Inc. Page 77 Manual No. M03-165-F0612SPINDLE ENTRY CODE SMC SRCT-D 94 200 0T-E 95 500 0T-F 96 1000 0ULA 00 0.64

Seite 78 - Table D-2

Brookeld Engineering Labs., Inc. Page 78 Manual No. M03-165-F0612Table D-2 lists the model codes and spring torque constants for each Viscomete

Seite 79 - +/-) 0.1°C

Brookeld Engineering Labs., Inc. Page 79 Manual No. M03-165-F0612Appendix E - Calibration ProceduresTheaccuracyoftheDV-II+Proisveriedus

Seite 80

Brookeld Engineering Labs., Inc. Page 8 Manual No. M03-165-F0612 I.2 UtilitiesInputVoltage: 115VACor230VACInputFrequency: 50/60HzPowe

Seite 81

Brookeld Engineering Labs., Inc. Page 80 Manual No. M03-165-F0612Brookeld Viscosity Standard Fluid General Information We recommendthatBrook

Seite 82 - +Pro Viscometer

Brookeld Engineering Labs., Inc. Page 81 Manual No. M03-165-F0612Calibration Procedure for a Small Sample Adapter Brookeldrecommendsatwost

Seite 83

Brookeld Engineering Labs., Inc. Page 82 Manual No. M03-165-F0612WhenaULorDINULAdapterisused,thewaterbathisstabilizedattheprope

Seite 84

Brookeld Engineering Labs., Inc. Page 83 Manual No. M03-165-F0612Calibration Procedure for Cone/Plate Viscometers 1) Follow the above procedur

Seite 85

Brookeld Engineering Labs., Inc. Page 84 Manual No. M03-165-F0612Sample Adapter, UL Adapter, Thermosel, Spiral Adapter, and DIN Adapter the acc

Seite 86

Brookeld Engineering Labs., Inc. Page 85 Manual No. M03-165-F06122) TheViscosityStandardFluidis101.5cP.Itsaccuracyis:  +/-1%x10

Seite 87 - For LV Torque

Brookeld Engineering Labs., Inc. Page 86 Manual No. M03-165-F0612Appendix F - The Brookeld GuardlegTheguardlegwasoriginallydesignedtopr

Seite 88 - Appendix G - Speed Sets

Brookeld Engineering Labs., Inc. Page 87 Manual No. M03-165-F0612should be known that this type of torque reading will not convert into a corre

Seite 89 - Appendix H - Communications

Brookeld Engineering Labs., Inc. Page 88 Manual No. M03-165-F0612Appendix G - Speed SetsThe following speed sets and custom speeds are selectab

Seite 90

Brookeld Engineering Labs., Inc. Page 89 Manual No. M03-165-F0612Appendix H - CommunicationsWhenusingtheBrookeld ComputerCable (Brookel

Seite 91 - Figure I-1

Brookeld Engineering Labs., Inc. Page 9 Manual No. M03-165-F0612Temperature Accuracy: ±1°C|-100°Cto+149°C ±2°C|+150°Cto+300°COper

Seite 92

Brookeld Engineering Labs., Inc. Page 90 Manual No. M03-165-F0612234567891No ConnectionTransmit Data (TxD)No ConnectionHigh Speed Print(Note 1)

Seite 93 - Figure J-3

Brookeld Engineering Labs., Inc. Page 91 Manual No. M03-165-F0612Appendix I - Model S Laboratory Stands4CLAMP ASSEMBLYNOTE: “FRONT” FACES TOWAR

Seite 94

Brookeld Engineering Labs., Inc. Page 92 Manual No. M03-165-F0612UnpackingCheck carefully to see that all the components are received with no c

Seite 95 - No Recorder Response

Brookeld Engineering Labs., Inc. Page 93 Manual No. M03-165-F0612Appendix J - DVE-50A Probe ClipProbe Clip DVE-50A is supplied with all model D

Seite 96

Brookeld Engineering Labs., Inc. Page 94 Manual No. M03-165-F0612Appendix K -Fault Diagnosis and Troubleshooting Listed are some of the more co

Seite 97 - TURN POWER OFF

Brookeld Engineering Labs., Inc. Page 95 Manual No. M03-165-F0612❏ Viscometer Will Not Return to Zero ✓ Viscometer is not level  • Chec

Seite 98

Brookeld Engineering Labs., Inc. Page 96 Manual No. M03-165-F0612❏ Recorder Pen Moves in Wrong Direction ✓ Output polarity reversed  • R

Seite 99

Brookeld Engineering Labs., Inc. Page 97 Manual No. M03-165-F0612Timed Stop Minutes 01 Seconds 30 RPM 50Time to Torque Torque % 60 RPM 5

Seite 100 - Warranty

Brookeld Engineering Labs., Inc. Page 98 Manual No. M03-165-F0612Appendix L - Instrument Dimensions13 21/64”[33.9 cm]7 15/16”[20.2 cm]4 9/64”[1

Seite 101 - VISCOSITY TEST REPORT

Brookeld Engineering Labs., Inc. Page 99 Manual No. M03-165-F0612Appendix M - Online Help and Additional Resourceswww.brookeldengineering.com*

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